期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 75, 期 12, 页码 4183-4191出版社
AMER CHEMICAL SOC
DOI: 10.1021/jo100618d
关键词
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资金
- Ministry of Education, Science and Technology [2009-0066777]
- National Research Foundation of Korea [2009-0066777] Funding Source: Korea Institute of Science & Technology Information (KISTI), National Science & Technology Information Service (NTIS)
Novel 1,3-dialkyl-1,2,3-triazolium ionic liquids were synthesized via click reactions using 1-trimethylsilylacetylene and alkyl azides and were efficient reaction media for the Baylis-Hillman reaction. The problems associated with deprotonation of the C-2 hydrogen of [bmim][PF(6)] could be suppressed in the reaction of [bmTr][PF(6)] or [bmTr][NTf(2)]. 1,3-Dialkyl-1,2,3-triazolium ionic liquids are chemically inert under basic conditions and more suitable media for the reactions involving bases than the common 1,3-dialkylimidazolium ionic liquids.
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