期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 75, 期 15, 页码 5289-5295出版社
AMER CHEMICAL SOC
DOI: 10.1021/jo101226r
关键词
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资金
- NSFC [20732002, 20921120404, 20972059]
- MOST [2010CB833203]
- MOE
A new one-pot procedure for the preparation of aminoenone from chloroalkyl enone and sodium azide was demonstrated. The structure of the presumed triazoline intermediate in this process was confirmed by X-ray analysis for the first time. As the application of this methodology, the synthesis of polycyclic alkaloid hexahydroapoerysopine (1a) was achieved through an efficient synthetic route.
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