期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 73, 期 9, 页码 3658-3661出版社
AMER CHEMICAL SOC
DOI: 10.1021/jo800328a
关键词
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[GRAPHICS] A novel and selective method for the synthesis of 8-methylenespiro[4,5]trienes via intramolecular electrophilic ipsoiodocyclization of N-(4-methylphenyl)propiolamides has been developed. In the presence of ICI or I-2, 8-methylene-1-azaspiro[4,5]trienes were selectively prepared from the electrophilic ipso-iodocyclization of N-(4-methylphenyl)propiolamides in moderate to good yields.
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