期刊
JOURNAL OF NON-CRYSTALLINE SOLIDS
卷 384, 期 -, 页码 83-87出版社
ELSEVIER SCIENCE BV
DOI: 10.1016/j.jnoncrysol.2013.07.021
关键词
X-ray absorption spectroscopy; Oxyfluoride glass-ceramics; Fluoride crystals; Rare earths
Incorporation of rare-earth (RE) ions in the fluoride crystals of oxyfluoride glass-ceramics greatly improves the optical properties of these materials, such as the up-conversion emission. In this work, we present a study of this incorporation using X-ray absorption near-edge structure (XANES) spectroscopy and extended X-ray absorption fine structure (EXAFS) spectroscopy. Both techniques allow quantifying the distribution of these ions in the glass matrix and the fluoride crystals. We found that 27% of Tm3+ ions are incorporated in LaF3 nano-crystals. (C) 2013 Elsevier B.V. All rights reserved.
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