4.2 Article

Preparation of α-Fe2O3 Nanotubes by Calcination of Electrospun Precursors

期刊

JOURNAL OF NANOSCIENCE AND NANOTECHNOLOGY
卷 14, 期 3, 页码 2670-2673

出版社

AMER SCIENTIFIC PUBLISHERS
DOI: 10.1166/jnn.2014.8477

关键词

alpha-Fe2O3; Nanotube; Electrospinning; Morphology; Preparation

资金

  1. National Natural Science Foundation of China [51274106]
  2. Science and Technology Support Program of Jiangsu Province [BE2012143]
  3. Natural Science Research Program of Jiangsu Province Higher Education [12KJA430001]
  4. Natural Science Research Program of Jiangsu Province [BK2010334]
  5. Jiangsu Province's Postgraduate Cultivation and Innovation Project [CXZZ11_0557]
  6. Science and Technology Support Project of Zhenjiang [SH2012026]
  7. Jiangsu University Students Research Projects [11A142]
  8. Priority Academic Program Development of Jiangsu Higher Education Institutions

向作者/读者索取更多资源

The alpha-Fe2O3 nanotubes with diameters of 400-700 nm were prepared by calcination of electrospun precursors. The morphology of alpha-Fe2O3 nanotubes is mainly influenced by the water content in solution and heating rate during the calcination process. When the water content is about 17 wt.%, heating rate is 5 degrees C/min and calcination temperature at 500 degrees C for 2 h, the optimized alpha-Fe2O3 nanotubes are obtained. These alpha-Fe2O3 nanotubes have a magnetization (M-s) of 0.36 emu . g(-1) and coercivity (H-c) of 1942 Oe and can be used in the nanospace technology.

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