期刊
JOURNAL OF NANOMATERIALS
卷 2014, 期 -, 页码 -出版社
HINDAWI LTD
DOI: 10.1155/2014/289150
关键词
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资金
- Faculty of Science, University of Johannesburg
- National Research Fund (NRF) South Africa
- Nanotechnology and Applications Centre, University of Allahabad, Allahabad, India
A series of S/Gd3+-codoped TiO2 photocatalysts were synthesized by a modified sol-gel method. The materials were characterized by X-ray diffraction (XRD), Raman spectroscopy, Fourier transform infrared spectroscopy (FTIR), UV-visible diffuse reflectance spectroscopy, scanning electron microscopy (SEM)/energy-dispersive X-ray spectroscopy (EDX), and transmission electron microscopy (TEM)/energy-dispersive spectroscopy (EDS). Laboratory experiments with Indigo Carmine chosen as a model for organic pollutants were used to evaluate the photocatalytic performance of S/Gd3+-codoped TiO2 under visible-light with varying concentrations of Gd3+ ions in the host material. XRD and Raman results confirmed the existence of anatase phase TiO2 with particle size ranging from 5 to 12 nm. Codoping has exerted a great influence on the optical responses along with red shift in the absorption edge. S/Gd3+-codoped TiO2 showed significant visible-light induced photocatalytic activity towards Indigo Carmine dye compared with S-TiO2 or commercial TiO2. TiO2-S/Gd3+ (0.6% Gd3+) degraded the dye (k(a) = 5.6 x 10(-2) min(-1)) completely in 50 min.
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