期刊
ORGANIC LETTERS
卷 17, 期 4, 页码 876-879出版社
AMER CHEMICAL SOC
DOI: 10.1021/ol5037387
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资金
- National Basic Research Program of China (973 Program) [2015CB856600]
- National Natural Science Foundation of China [21325206, 21172006]
- National Young Top-notch Talent Support Program
An efficient method for the direct preparation of high synthetic valuable a-hydroxycarbonyls is described. The simple and readily available I-2 or NBS was used as catalyst. DMSO acts as the oxidant, oxygen source, and solvent. A diverse range of tertiary Csp(3)-H bonds as well as more challenging secondary Csp(3)-H bonds could be hydroxylated in this transformation. The reaction is mild, less toxic and easy to perform.
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