期刊
JOURNAL OF ELECTRON MICROSCOPY
卷 58, 期 6, 页码 331-339出版社
OXFORD UNIV PRESS
DOI: 10.1093/jmicro/dfp028
关键词
environmental TEM; gas reaction; high temperature; high resolution; oxidation; reduction
类别
Many automotive materials, such as catalysts and fuel cell materials, undergo significant changes in structure or properties when subjected to temperature change or the addition of a gas. For this reason, in the development of these materials, it is important to study the behavior of the material under controlled temperatures and gaseous atmospheres. Recently, a new environmental transmission electron microscope (TEM) has been developed for observation with a high resolution at high temperatures and under gaseous atmospheres, thus making it possible to analyze reaction processes in details. Also, the new TEM provides a high degree of reproducibility of observation conditions, thus making it possible to compare and validate observation of various specimens under a given set of conditions. Furthermore, easiness of gas condition and temperature control can provide a powerful tool for the studying of the mechanism of material change, such as oxidation and reduction reactions.
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