Article
Chemistry, Analytical
Julia Kazakova, Mercedes Villar-Navarro, Juan Luis Perez-Bernal, Maria Ramos-Payan, Miguel Angel Bello-Lopez, Rut Fernandez-Torres
Summary: This study proposed a method for the determination of 2,4-, 2,5-, and 2,6-dinitrophenols and some of their metabolites in human urine and saliva. By using liquid phase microextraction coupled with ultra-high performance liquid chromatography-quadrupole time-of-flight mass spectrometry, low detection and quantitation limits of the target analytes were achieved, allowing the investigation and tentative identification of metabolites.
MICROCHEMICAL JOURNAL
(2021)
Article
Biochemistry & Molecular Biology
Roziana Kamaludin, Lubna Abdul Majid, Mohd Hafiz Dzarfan Othman, Sumarni Mansur, Siti Hamimah Sheikh Abdul Kadir, Keng Yinn Wong, Watsa Khongnakorn, Mohd Hafiz Puteh
Summary: The study fabricated antibacterial hollow fiber membranes with zinc oxide nanoparticles, improving membrane anti-biofouling characteristics and achieving good pure water flux and protein rejection rate.
Article
Chemistry, Physical
Reza Hoseinpour Kouhestany, Atefeh Tamaddon, Homayon Ahmad Panahi, Arash Afshar Ebrahimi, Rahebeh Amiri
Summary: Researchers synthesized novel hyperbranched dendrimers grafted on SiO2 nanoparticles as nanosorbents for the trace extraction of exemestane. They optimized the parameters for adsorption efficiency and achieved a lower detection limit by using the HF-LPME system. The proposed method, combined with high-performance liquid chromatography, successfully determined exemestane in biological and pharmaceutical samples.
JOURNAL OF MOLECULAR LIQUIDS
(2023)
Article
Materials Science, Multidisciplinary
Carlos Hernandez, Santosh K. Gupta, Jose P. Zuniga, Jorge Vidal, Rene Galvan, Hector Guzman, Lilian Chavez, Karen Lozano, Yuanbing Mao
Summary: In this study, flexible PVDF fibrous mats doped with Eu3+ sources were developed using Forcespinning method. The high-pressure optical properties of Eu3+ ions in EN-PF and ES-PF were investigated, showing different extent of changes in their characteristics with increasing pressure. Irreversible changes were observed in both Eu3+ doped PVDF systems under high-pressure conditions, presenting opportunities for multifunctional applications.
JOURNAL OF MATERIALS SCIENCE & TECHNOLOGY
(2021)
Article
Engineering, Environmental
Yunus Aksoy, Halil Hasar
Summary: The study demonstrated the usability of gas-permeable hollow fiber membranes produced with additives in a membrane biofilm reactor. These membranes showed increased oxygen gas diffusion coefficients, leading to improved nitrate reduction and ammonium oxidation. This cost-effective approach could help promote membrane biofilm technology.
JOURNAL OF WATER PROCESS ENGINEERING
(2021)
Article
Engineering, Chemical
Murong Yang, Haihui Liu, Kaikai Chen, Mianning Wang, Huanhuan Chen, Wei Zhao, Changfa Xiao
Summary: Membrane separation technology is widely used in various fields, especially in water treatment. A study focuses on the preparation of PVDF hollow fiber composite membranes through a green preparation method. The addition of PEO promotes phase separation and improves membrane performance. The prepared membrane shows high water flux, excellent protein rejection, and strong mechanical properties.
JOURNAL OF THE TAIWAN INSTITUTE OF CHEMICAL ENGINEERS
(2023)
Article
Chemistry, Analytical
Leyla Haidari-Khoshkelat, Jahan Bakhsh Raoof, Milad Ghani, Reza Ojani
Summary: In this study, a combination of two extraction techniques was used to analyze antibiotics in water and urine samples. The method was found to accurately quantify the selected analytes and was applicable to complex biological samples.
ANALYTICA CHIMICA ACTA
(2022)
Article
Engineering, Multidisciplinary
Jung-Eun Lee, Young-Eun Shin, Ga-Hyeun Lee, Jihyun Kim, Hyunhyub Ko, Han Gi Chae
Summary: PVDF/CNC nanocomposite fibers with good mechanical properties and high beta phase fraction were prepared, suitable for smart textile applications. The tensile properties of all fibers were enhanced as the polymeric chains were extended during the stretching process. The optimal nanocomposite fiber was prepared with 1 wt% CNC loading.
COMPOSITES PART B-ENGINEERING
(2021)
Article
Biochemical Research Methods
Nerea Lorenzo-Parodi, Wiebke Kaziur-Cegla, Astrid Gjelstad, Torsten C. Schmidt
Summary: Aromatic amines, such as those found in tobacco smoke, can enter the human body and be excreted in urine. Hollow fiber-liquid-phase microextraction (HF-LPME) and parallel artificial liquid membrane extraction (PALME) were optimized as alternatives to traditional liquid-liquid extraction (LLE) for measuring these compounds. PALME showed significantly higher recovery rates compared to HF-LPME and was further validated for nine different aromatic amines. The results demonstrate that PALME is a greener, more efficient, and automated alternative to LLE.
ANALYTICAL AND BIOANALYTICAL CHEMISTRY
(2023)
Article
Engineering, Chemical
Zhan Li, Pengfei Zhang, Kecheng Guan, Tomohisa Yoshioka, Hideto Matsuyama
Summary: Vacuum membrane distillation (VMD) is an important technology for the production of high-purity water. Researchers have modified the membrane to improve its performance, resulting in increased water flux and improved hydrophobic properties.
Article
Environmental Sciences
Gizem Tuncay, Turker Turken, Ismail Koyuncu
Summary: In this study, braid reinforced membranes were fabricated using two different molecular weights of PVDF polymers. The blending of the polymers improved the membrane performance, resulting in a hydrophilic structure with a smoother surface. The investigation showed that the blend membrane had less adsorption of pollutants and reduced fouling.
ENVIRONMENTAL TECHNOLOGY
(2022)
Article
Chemistry, Multidisciplinary
Eskinder Teklu Bekele, S. Dube, M. M. Nindi
Summary: In this study, a three-phase hollow fibre-supported liquid membrane technique combined with high-performance liquid chromatography was developed for the analysis of sulfonamide residues in chicken egg samples. The method showed good performance in terms of extraction, clean-up, and determination, and has the potential to be used as an alternative method.
JOURNAL OF CHEMISTRY
(2022)
Article
Engineering, Chemical
Thi My Hanh Le, Rong Wang, Sermpong Sairiam
Summary: PVDF photocatalytic hollow fiber membranes coated with polydopamine (PDA) and titanium dioxide nano-particles (TiO2) were prepared to improve the long-term stability and performance durability for dye wastewater treatment. The PDA-treated membranes showed resistance to UV radiation, while the PVDF-TiO2 membrane without PDA pretreatment was destroyed after 9 days of continuous UV irradiation. The membranes treated with PDA and TiO2 exhibited significantly increased COD removal rate (above 60%) and stable permeate flux and dye rejection rate after 5 cycles (20 h of operation).
JOURNAL OF MEMBRANE SCIENCE
(2023)
Article
Nanoscience & Nanotechnology
Zhaohan Yu, Ming Chen, Yunming Wang, Jiaqi Zheng, Yongkang Zhang, Huamin Zhou, Dequn Li
Summary: The study introduces a novel piezo-tribo hybrid nanogenerator employing nanoporous PVDF hollow fiber and PDMS valve, mimicking the eardrum for efficient acoustic harvesting, achieving high energy conversion efficiency and power density.
ACS APPLIED MATERIALS & INTERFACES
(2021)
Article
Materials Science, Characterization & Testing
Jingjing Yan, Changfa Xiao, Dawei Ji
Summary: The PVDF hollow fiber membrane reinforced with homogeneous fibers prepared through dry-wet spinning process showed improved mechanical properties and separation performance. The fibers were evenly distributed in the separation layer and parallel to the membrane axis. The reinforcement mechanism and the potential to adjust membrane properties with different fiber structures were investigated.
Article
Chemistry, Inorganic & Nuclear
Yixuan Pang, Shuang Li, Huibin Wang, Ning Zhang, Ruipeng Chen, Cherie S. Tan, Yating Xia, Hui Zhao, Yuanqing Cao, Jun Liang
Summary: In this study, a novel strategy for detecting harmful amines migrated from packaging printing inks is presented. By competitive coordination substitution and electrostatic interactions, the fluorescence of the organic ligand is re-enhanced, enabling highly sensitive and selective detection of potentially harmful amines.
JOURNAL OF SOLID STATE CHEMISTRY
(2023)
Review
Chemistry, Analytical
Juan Zheng, Yixin Kuang, Suxin Zhou, Xinying Gong, Gangfeng Ouyang
ANALYTICAL CHEMISTRY
(2023)
Article
Environmental Sciences
Zizi Li, Zhi-Mei Luo, Yanjun Huang, Jia-Wei Wang, Gangfeng Ouyang
Summary: The elimination and restriction of PFOA and PFOS have led manufacturers to shift production to substitutes, which still pose threats to the environment. This review summarizes the progress in degrading these substitutes and discusses future prospects for optimization. Differences in the degradation of various substitutes are also discussed to derive designing principles for more degradable F-containing compounds.
Article
Chemistry, Physical
Yanjun Huang, Hao Dai, Dooshaye Moonshiram, Zhuofeng Li, Zhi-Mei Luo, Ji-Hong Zhang, Wenxing Yang, Yong Shen, Jia-Wei Wang, Gangfeng Ouyang
Summary: Metal complexes hybridized with conductive supports are desirable catalysts for CO2 electroreduction. In this study, a conjugation-tuning strategy was employed to improve both the intrinsic activity of the complex and the molecule-support interactions by comparing Ni(ii) octabutoxyphthalocyanine and Ni(ii) octabutoxynaphthalocyanine on multi-walled carbon nanotubes. The impaired conjugation in NiPc-B enhances both activity and molecule-support affinity, resulting in higher faradaic efficiencies for CO production compared to NiNc-B.
JOURNAL OF MATERIALS CHEMISTRY A
(2023)
Article
Chemistry, Multidisciplinary
Xinxing Lin, Xiaolin Wang, Hongyuan Cui, Ping Rao, Yuezhong Meng, Gangfeng Ouyang, Hui Guo
Summary: Bioinspired smart hydrogels with additive-switchable mechanical properties have been developed using a novel strategy to prepare additive-responsive hydrogels with highly tunable toughness under quasi-isochoric conditions. The softening transition temperature of the hydrogels is tuned through non-covalent interactions between polymer networks and additives. The mechanical behaviors of the hydrogels depend on the type and concentration of additives, and the regulation with additives shows satisfactory reversibility and universality.
MATERIALS HORIZONS
(2023)
Article
Biochemical Research Methods
Chang Hu, Ziyue Qin, Jie Fu, Qiya Gao, Chong Chen, Cherie S. Tan, Shuang Li
Summary: An aptamer-based electrochemical biosensor was constructed for sensitive detection of CA125. Molybdenum disulfide (MoS2) was used as the stable layered substrate, combined with the irregular branched structure of gold nanoflowers (AuNFs) to provide a large specific surface area. The sensor showed reasonable specificity, reproducibility, and stability, and was consistent with the gold standard in negative/positive judgment.
ANALYTICAL BIOCHEMISTRY
(2023)
Article
Biochemical Research Methods
Guosheng Chen, Siming Huang, Xiaomin Ma, Rongwei He, Gangfeng Ouyang
Summary: Enzymes, as exceptional natural catalysts, play vital roles in life-sustaining biotransformations due to their exquisite 3D structures. However, their flexibility makes them vulnerable in non-physiological environments, hindering their large-scale industrial applications. This study presents a new bottom-up strategy for enzyme encapsulation using a hydrogen-bonded organic framework (HOF-101), allowing for the encapsulation of various enzymes within a highly crystalline scaffold. Compared to other methods, this enzyme-triggering HOF-101 encapsulation is easy to operate and offers higher loading efficiency, with a well-arranged structure and mesochannels that enhance mass transfer and understanding of biocatalytic processes.
Article
Chemistry, Multidisciplinary
Haojun Li, Qingqing Jin, Haibo Li, Hua Tong, Keke Wang, Shuoran Chen, Gangfeng Ouyang, Zuankai Wang, Yanan Li
Summary: A scalable template-assisted spray coating method has been developed to fabricate highly transparent superamphiphobic materials. These materials eliminate visible-light scattering, maintain superamphiphobicity, and exhibit improved mechanical, chemical, and thermal stabilities. They can be applied on various substrates, showing enormous potential for various applications.
ADVANCED FUNCTIONAL MATERIALS
(2023)
Article
Chemistry, Analytical
Jing Guo, Lihua Wu, Yu-Xin Ye, Fang Zhu, Jianqiao Xu, Gangfeng Ouyang
Summary: Two-dimensional conductive metal-organic frameworks (cMOFs) have been used for electrochemical sensing, but their application in aqueous solutions is still in the early stage. In this study, the interfacial capacitances of a 2D cMOF are utilized for electrochemical sensing for the first time and successfully detect various compounds in aqueous solutions. The responses are rooted in the pseudocapacitances of the 2D cMOF, revealing deep insights into the response mechanisms and promoting the application of 2D cMOFs in chemical sensing.
ANALYTICAL CHEMISTRY
(2023)
Article
Chemistry, Analytical
Hongyu Wen, Minhui Shen, Zhisheng Lai, Xiaoru Peng, Yu-Xin Ye, Jianqiao Xu, Gangfeng Ouyang
Summary: This study presents a novel noncovalent tagging method integrated with mass spectrometry for identifying specific bioactive contaminants. By selecting a stereoselective hexapeptide as the tag through proteolysis, the contaminants that bind to dopamine receptors can be distinguished and analyzed using mass spectrometry. Using this method, the widely used additive 1,3-diphenylguanidine was successfully identified in Pearl River water and confirmed as a potential disrupter to dopamine receptors.
ANALYTICAL CHEMISTRY
(2023)
Article
Chemistry, Analytical
Chenchen Song, Juan Zheng, Qidong Zhang, Hang Yuan, Ajuan Yu, Wenfen Zhang, Shusheng Zhang, Gangfeng Ouyang
Summary: The contamination of surface and ground water by PFASs is a growing concern. A method for monitoring coexistent PFASs at trace levels in aquatic environments is urgently needed. In this study, COF-NH-CO-F9 was successfully synthesized and used for the extraction of broad-spectrum PFASs, enabling the development of a highly efficient and sensitive method using SPME and UHPLC-MS/MS. The method demonstrated high enrichment factors, ultrahigh sensitivity, wide linearity, and satisfactory precision, with successful application in real water samples.
ANALYTICAL CHEMISTRY
(2023)
Article
Materials Science, Multidisciplinary
Hua Tong, Zhennan Zhou, Yi Lv, Haibo Li, Wei Liu, Gangfeng Ouyang
Summary: An efficient method has been developed to prepare copper(I) iodide incorporated organic-inorganic hybrid coating materials. These materials have the potential to be solvent-free anti-counterfeiting inks, offering advantages of easy preparation, low cost, uniform and bright light emissions, long service life, high stability, water resistance, and strong wearability.
MATERIALS ADVANCES
(2023)
Article
Chemistry, Multidisciplinary
Anlian Huang, Linjing Tong, Xiaoxue Kou, Rui Gao, Zhi-Wei Li, Siming Huang, Fang Zhu, Guosheng Chen, Gangfeng Ouyang
Summary: This contribution comprehensively investigates the biomineralization of zeolite imidazole frameworks for one-step synthesis of an enzyme-MOF biocomposite. The study reveals that the biomineralization ability depends on the ZIF organic linker, and the biocatalytic function is highly related to the ZIF mineral species and their microstructures. Additionally, the protective effect of ZIF mineral on the hosted enzyme is associated with the synergistic effect of size dimension and chemical microenvironment of the ZIF pores.
Review
Chemistry, Physical
Zeyu Gong, Jiaxing Yu, Linjing Tong, Yu Hou, Huajie Zhong, Yuan Tao, Guosheng Chen, Junhui Wang, Fang Zhu, Gangfeng Ouyang
Summary: This article provides a comprehensive overview of the latest advances in solar-driven metal-free catalysts for water disinfection. It focuses on the development of metal-free photocatalysts, their physical and chemical properties, and the role of active species. The research progress of photocatalytic reactors in microbial inactivation is highlighted to promote the large-scale application of photocatalysis in practical industry.
CATALYSIS SCIENCE & TECHNOLOGY
(2023)
Article
Chemistry, Multidisciplinary
Yueru Shi, Ruolun Xu, Shaohan Wang, Juan Zheng, Fang Zhu, Qingkun Hu, Junlong Huang, Gangfeng Ouyang
Summary: Synthetic cannabinoids (SCs) have emerged as a significant public health threat worldwide. In this study, a highly selective covalent organic framework (FSQ-4) was synthesized to efficiently enrich different SCs. Coupled with solid-phase microextraction, trace-level determination of 13 SCs can be easily achieved.
Correction
Biochemical Research Methods
Yong Wang, Suhua Yu, Rui Li, Jing Wan, Yuheng Wang, Zongli Huo, Chunyong Wu, Li Mi, Songqin Liu
JOURNAL OF CHROMATOGRAPHY A
(2024)
Review
Biochemical Research Methods
Israel D. Souza, Maria Eugenia C. Queiroz
Summary: Organic-silica hybrid monolithic materials have gained significant attention in separation science and sample preparation due to their unique properties. This review summarizes the characteristics, current status, and recent developments of these materials, as well as discusses synthesis methods, characterization techniques, and strategies for improving extraction efficiency in various applications.
JOURNAL OF CHROMATOGRAPHY A
(2024)
Article
Biochemical Research Methods
Bhagwat Upreti, Bhanu Prasad Vempatapu, Jagdish Kumar, Pankaj K. Kanaujia
Summary: Lubricating oils are essential for the effective performance of internal combustion engines. This study presents a new HPLC method for determining additives in finished lubricating oils and polar substances in used engine oils.
JOURNAL OF CHROMATOGRAPHY A
(2024)
Article
Biochemical Research Methods
Zongqing Huang, Haoju Hua, Xiuzhen Du, Zipeng Zhen, Wei Zhao, Jun Feng, Ji-an Li
Summary: This study successfully isolated VHHs against the SUMO protein for the first time using biopanning of an immune camelid nanobody library. The VHHs were coupled to agarose resins to form affinity chromatography resins, allowing for one-step purification of various SUMO fusions.
JOURNAL OF CHROMATOGRAPHY A
(2024)
Article
Biochemical Research Methods
Xueting Qiu, Xuben Hou, Yue Yang, Hao Fang, Fei Cui, Xinying Yang
Summary: In this study, a new method based on electrophoretically mediated microanalysis was developed for the investigation of PTPRO enzymatic activity. The method was successfully used to determine the kinetics of PTPRO and the inhibitory concentration of PTPRO inhibitors. The method exhibited improved accuracy and reduced consumption compared to traditional methods.
JOURNAL OF CHROMATOGRAPHY A
(2024)
Article
Biochemical Research Methods
Feifei Luo, Mengmeng Hao, Lei Zhang, Yangguo Xie, Wei Hou, Hongya Wang, Zhongli Zhang
Summary: In this study, a comprehensive screening and structure elucidation of 23 nonvolatile organic compounds (NVOCs) in two antibody drugs was conducted. Seven previously unreported compounds were identified. A quantitative method with high sensitivity, accuracy, and precision was developed for evaluating the safety of NVOCs in drug products.
JOURNAL OF CHROMATOGRAPHY A
(2024)
Article
Biochemical Research Methods
Zuzana Vosahlova, Kveta Kalfkova, Martin Gilar, Jakub Szymarek, Maria Mazurkiewicz-Beldzinska, Sylwia Studzi
Summary: A hydrophilic interaction liquid chromatography method was developed for the separation and identification of oligonucleotide impurities and metabolites, and successfully applied to the analysis of serum samples from Spinraza-treated patients.
JOURNAL OF CHROMATOGRAPHY A
(2024)
Article
Biochemical Research Methods
Aswanidevi Kongasseri, Thirumalai Madhesan, Sangeetha Krishna Kumar, Sushmitha Pedugu Sivaraman, Suchashrita Mitra, Pitchaiah Kancharlapalli Chinaraga, C. V. S. Brahmmananda Rao, Sivaraman Nagarajan, Prabhakaran Deivasigamani, Akhila Maheswari Mohan
Summary: This study focuses on the sequential separation of trivalent lanthanides using modified C-18 silica-packed supports and reversed-phase HPLC technique. By tuning the column modifiers and separation parameters, the researchers achieved systematic separation of Ln(3+). The results showed that the choice of column modifiers and fine-tuning of the modification procedure were crucial for achieving excellent separation.
JOURNAL OF CHROMATOGRAPHY A
(2024)
Article
Biochemical Research Methods
Raquel Perez-Robles, Szabolcs Fekete, Robert Kormany, Natalia Navas, Davy Guillarme
Summary: There is a mismatch between the sample diluent and the mobile phase in HILIC analysis, leading to analyte breakthrough and peak distortion. Adding a weak solvent for pre-injection can effectively prevent these issues and improve sensitivity.
JOURNAL OF CHROMATOGRAPHY A
(2024)
Article
Biochemical Research Methods
Oleg Pokrovskiy, Irina Rostovschikova, Konstantin Ustinovich, Ilya Voronov, Dmitry Kosyakov
Summary: A chromatography-like propagation of water through the material bed was observed during supercritical fluid extraction of aroma plants with high moisture content, which could be significant for modeling the kinetics of supercritical fluid extraction of non-volatile compounds.
JOURNAL OF CHROMATOGRAPHY A
(2024)
Article
Biochemical Research Methods
Yasar Kemal Recepoglu, Ozguer Arar, Asli Yuksel
Summary: Biosorption using phosphorylated hazelnut shell waste (FHS) is a promising method for lithium removal and recovery. This study investigated the performance of a continuous-flow packed-bed column system using FHS for ultra-low level lithium removal. The results showed that the lihium biosorption capacity of the FHS column was unaffected by the bed height, but decreased with increasing flow rate.
JOURNAL OF CHROMATOGRAPHY A
(2024)
Article
Biochemical Research Methods
Jian Sun, Zheheng Zheng, Zixiao Jia, Jiabin Wang, Xucong Lin
Summary: In this study, an ionic covalent organic framework (iCOF) surface grafting monolithic sorbent was prepared for in-tube solid-phase microextraction (SPME) of aristolochic acids (AAs) in various samples. The density of quaternary ammonium ions in the iCOF was modulated for enhanced adsorption of AAs. The iCOF surface grafting monolithic sorbent was confirmed by different means. Several operating conditions were optimized to develop the online in-tube SPME-HPLC method, which showed good linearity, low limits of detection, and high recoveries for AAs in serum samples. This study presents a feasible approach for the application of COF-based monolithic sorbents in sample preparation.
JOURNAL OF CHROMATOGRAPHY A
(2024)
Article
Biochemical Research Methods
Zeng Wen, Ruihan Peng, Die Gao, Jing Lin, Jia Zeng, Zhou Li, Famin Ke, Zhining Xia, Dandan Wang
Summary: A chitosan-alginate sponge with multiple cross-linking networks was developed for adsorption and enrichment of anionic dyes from food samples. The sponge showed better three-dimensional network structure, mechanical behavior, and stability compared to pure chitosan and alginate sponges. The adsorption performance and selectivity of the sponge were systematically studied, and it maintained high adsorption capacity and selectivity for anionic dyes. The sponge also showed satisfactory reusability and was successfully combined with high-performance liquid chromatography for the enrichment and detection of anionic dyes in candy and cocktail samples.
JOURNAL OF CHROMATOGRAPHY A
(2024)
Article
Biochemical Research Methods
Hairong Zhang, Xiaojuan Jiang, Dandan Zhang, Yuexin Yang, Qiang Xie, Caisheng Wu
Summary: Analysis of in vivo exposure to traditional Chinese medicine using mass spectrometry is helpful for identifying effective ingredients and developing new drugs. This study focused on Forsythia suspensa (Lian Qiao) and used metabolomics technology to explore its in vivo exposure. By comparing the differences before and after administration, a complete set of nontargeted analysis strategies for TCM exposure was established. The study identified 393 Lian Qiao-related chemical components in mice after administration, including prototypes and metabolites. This study provides a reference for research on the active ingredients of Lian Qiao in vivo.
JOURNAL OF CHROMATOGRAPHY A
(2024)
Article
Biochemical Research Methods
Oscar Castejon-Musulen, Ricardo Lopez, Ignacio Ontan, Vicente Ferreira
Summary: A quantitative analytical method was developed and validated in this study to determine the concentrations of 81 aroma-relevant wine volatiles. The method utilizes stir bar sorptive extraction and multidimensional gas chromatography with flame ionization detector or mass spectrometer. The method demonstrated good linearity, reproducibility, and recovery, and was successfully applied to analyze 20 wine samples.
JOURNAL OF CHROMATOGRAPHY A
(2024)