期刊
JOURNAL OF AOAC INTERNATIONAL
卷 95, 期 3, 页码 913-922出版社
OXFORD UNIV PRESS INC
DOI: 10.5740/jaoacint.11-140
关键词
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资金
- Sao Paulo Research Foundation (FAPESP)
- Coordination for the Improvement of Higher Level Education Personnel (CAPES)
- National Council for Scientific and Technological Development (CNPq)
A simple method using LC/MS/MS was developed and validated to determine residues of malachite green (MG) and leucomalachite green (LMG) in fish fillet. A modified QuEChERS (Quick, Easy, Cheap, Effective, Rugged, and Safe) technique was used to perform the sample preparation. The optimal extraction and cleanup conditions were established using an experimental design. The validation parameters obtained to determine both MG and LMG complied with the requirements established by regulatory agencies for the presence of such substances in fish, which establish that the method must attain, at least, a minimum required performance limit of 2 ng/g. The accuracy values ranged between 95 and 107%, and the precision values were lower than 11.2%. The method was used in the analysis of tilapia samples (n = 20) commercialized in Campinas, SP, Brazil. None of the samples presented detectable levels of MG or LMG residues.
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