4.7 Article

Synthesis of ZnS nanoparticles via hydrothermal process assisted by microemulsion technique

期刊

JOURNAL OF ALLOYS AND COMPOUNDS
卷 486, 期 1-2, 页码 L40-L43

出版社

ELSEVIER SCIENCE SA
DOI: 10.1016/j.jallcom.2009.07.109

关键词

ZnS nanoparticles; Microemulsion technique; Hydrothermal process

资金

  1. National Natural Science Foundation of China [50772105]

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Uniform and spherical ZnS nanoparticles with a diameter of 5-10 nm were successfully synthesized at 160 degrees C via a facile hydrothermal process, where ZnS precursors were prepared by a microemulsion technique. The products were characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM), and photoluminescent (PL) spectra techniques, respectively. The results showed that the hydrothermal temperature exerted a more important effect than the holding time on the crystallization of ZnS crystallites. The as-prepared ZnS nanoparticles exhibited higher PL intensity than that of the normal ones of micrometer scale besides an obvious blue shift. (C) 2009 Elsevier B.V. All rights reserved.

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