期刊
MENDELEEV COMMUNICATIONS
卷 25, 期 6, 页码 415-416出版社
ELSEVIER SCIENCE BV
DOI: 10.1016/j.mencom.2015.11.004
关键词
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资金
- Russian Science Foundation [14-50-00126]
- Russian Foundation for Basic Research [15-33-20536]
- St. Petersburg State University [0.50.1186.2014]
Calcium carbide was studied as a useful solid-state reagent to incorporate acetylene unit into synthetic procedures. Atom-economic thiol-yne click reaction was successfully performed with single and double additions. Heterocyclic thiols and aliphatic dithiols reacted with acetylene generated in situ from calcium carbide to afford corresponding vinyl sulfides and bis(thiovinyl)ethers in good to high yields.
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