Article
Chemistry, Inorganic & Nuclear
Hui Dan, Li Chen, Zhen Li, Xinmiao He, Yi Ding
Summary: Amorphous ZrO2 powders were successfully prepared using a novel hydrothermal-assisted sol-gel method. The obtained powders exhibited features of small and uniform particle size, as well as high purity.
INORGANIC CHEMISTRY COMMUNICATIONS
(2022)
Article
Biochemistry & Molecular Biology
Michael S. Westphall, Kenneth W. Lee, Austin Z. Salome, Joshua J. Coon, Timothy Grant
Summary: Single-particle cryoEM has become a mature technique for structure determination in structural biology. However, the traditional plunge-freezing method used for preparing cryoEM grids still has limitations. The use of native mass spectrometry to create cryoEM samples offers a potential solution by avoiding sample damage and orientation issues. Although there are uncertainties and challenges, the combination of cryoEM and mass spectrometry shows great promise.
CURRENT OPINION IN STRUCTURAL BIOLOGY
(2023)
Article
Materials Science, Ceramics
S. Swathi, R. Yuvakkumar, G. Ravi, P. Kumar, S. Hong, Omaima Nasif, Sulaiman Ali Alharbi, Dhayalan Velauthapillai
Summary: Tantalum oxide is utilized for water splitting, with Ta2O5 nanopowders produced using the sol-gel process. The calcination time significantly impacts the crystal structure of Ta2O5, leading to different specific capacitance and current density values of Ta2O5 electrodes under various temperature conditions.
CERAMICS INTERNATIONAL
(2021)
Article
Nanoscience & Nanotechnology
Feng Qin, Feihu Chen, Junhua Hou, Wenjun Lu, Shaohua Chen, Jianjun Li
Summary: Plastic instability in strong multilayered composites is completely suppressed by architecting nanoscale BCC Nb crystalline-amorphous CuNb interfaces.
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING
(2024)
Article
Chemistry, Multidisciplinary
Christopher Leist, Ute Kaiser, Haoyuan Qi, Meng He, Xue Liu
Summary: Aberration-corrected transmission electron microscopy allows atomic resolution imaging of two-dimensional (2D) materials. This study successfully imaged carbon-based 2D materials with strong contrast, using chromatic and spherical aberration correction at a low acceleration voltage. A deep learning pipeline was constructed to accurately determine atomic registry in amorphous 2D materials, providing quantitative data sets.
Article
Materials Science, Ceramics
A. Zaborowska, L. Kurpaska, M. Clozel, E. J. Olivier, J. H. O'Connell, M. Vanazzi, F. Di Fonzo, A. Azarov, I Jozwik, M. Frelek-Kozak, R. Diduszko, J. H. Neethling, J. Jagielski
Summary: This study assessed the structural and mechanical properties of a 1 μm thick Al2O3 coating deposited on 316L stainless steel by Pulsed Laser Deposition (PLD) under high energy ion irradiation. The findings showed a slight reduction in hardness of all irradiated layers, but the irradiated layer remained amorphous. Comprehensive characterization techniques revealed excellent radiation resistance of alumina coatings under the given irradiation conditions.
CERAMICS INTERNATIONAL
(2021)
Article
Materials Science, Ceramics
K. Park, H. Kim, S. Y. Gwon, G. W. Jung, S. W. Kim
Summary: Phosphors of Lu2.94Al5O12:0.06Ce3+ prepared via a sol-gel process showed significantly enhanced photoluminescence properties under different synthesizing temperatures and fluoride fluxes, resulting in green-yellow emissions due to Ce3+ transitions. Among them, the 6 wt% BaF2-added Lu2.94Al5O12:0.06Ce3+ phosphor synthesized at 1400 degrees C exhibited the highest emission intensity, 173% stronger than that of the flux-free phosphor.
CERAMICS INTERNATIONAL
(2022)
Article
Chemistry, Physical
Aida Jover, Jacobo Troncoso, Maria Chiara di Gregorio, Francisco Fraga Lopez
Summary: The thermodynamics of the transition between two supramolecular aggregates of sodium deoxycholate in aqueous solution were characterized in this study. The morphological transition between the two structures was observed using electron microscopy. The results indicated that the transition process was influenced by factors such as temperature, pH, and surfactant concentration.
JOURNAL OF MOLECULAR LIQUIDS
(2022)
Article
Chemistry, Physical
Cheng-You Li, Tsung-Hsien Hsu, Cheng-Liang Huang
Summary: Amorphous Ce2Ti2O7 (CTO) thin films were prepared on an ITO/glass substrate using the sol-gel method, and the effects of various factors on the resistance-switching characteristics of the device were studied. It was observed that diffusion of Al and self-formed AlOx at the Al/CTO interface enhance the performance of the device. By inserting an AlOx layer at the CTO/ITO interface, the RS properties of the device can be optimized, making it a promising candidate for RRAM applications.
JOURNAL OF ALLOYS AND COMPOUNDS
(2023)
Article
Chemistry, Physical
Greta Inkrataite, Meldra Kemere, Anatolijs Sarakovskis, Ramunas Skaudzius
Summary: This study investigated the impact of boron doping on YAG, YLuAG, and LuAG materials, showing that the addition of boron can indeed shorten decay time and increase emission intensity. Powder compounds containing 1% and 5% boron exhibited the most intense emission, while pure samples doped with 5% boron showed the shortest decay times.
JOURNAL OF ALLOYS AND COMPOUNDS
(2021)
Article
Optics
R. Kokate, Pooja Rohilla, Sumandeep Kaur, A. S. Rao, Vijay Singh
Summary: The citrate sol-gel method was successfully used to synthesize a range of trivalent terbium phosphors, and their structural and performance characteristics were analyzed using various techniques. The results confirmed the material's excellent green emission properties, showcasing its potential as a green emitter for lighting applications.
Article
Chemistry, Physical
Mingyue Sun, Jinshui Xu, Jinyuan Ma, Ge Xu
Summary: An amorphous TiO2 nanoparticle (8-AT) was prepared via sol-gel method with pH adjustment to 8 using ammonia. The 8-AT had a particle size of 20-24 nm and specific surface area of 365.68 m2/g. It showed higher degradation efficiency for tetracycline (TC) compared to anatase TiO2 and P25, achieving 93.9% degradation within 30 minutes in dark reaction and 60 minutes under visible light irradiation. The study proposed a possible degradation mechanism based on the adsorption-photocatalytic activity of 8-AT.
JOURNAL OF ALLOYS AND COMPOUNDS
(2023)
Article
Chemistry, Multidisciplinary
Yanhui Wang, Maroua Bouchneb, Rimeh Mighri, Johan G. Alauzun, P. Hubert Mutin
Summary: Various non-hydrolytic sol-gel synthesis methods were investigated to selectively produce mesoporous t-ZrO2 or m-ZrO2 with significant specific surface areas. The presence of significant amounts of water favored the formation of m-ZrO2, while strictly non-hydrolytic routes favored the formation of t-ZrO2. The role of water in the structure of zirconia was found to be crucial.
CHEMISTRY-A EUROPEAN JOURNAL
(2021)
Article
Physics, Condensed Matter
Chien-Yie Tsay, Yun-Chi Chen, Hsuan-Meng Tsai, Cheng-Liang Hsu
Summary: Solar-blind ultraviolet photodetectors with an amorphous zinc-tin oxide sensing layer were fabricated and the effects of asymmetry ratio of a pair of aluminum interdigitated electrodes on the photoelectrical characteristics were investigated. The experimental results showed that the photodetectors had the best responsivity and specific detectivity when the asymmetry ratio was 10:1.
PHYSICA B-CONDENSED MATTER
(2022)
Article
Materials Science, Coatings & Films
Sayyed Ahad Sajjadi, Naghi Parvini Ahmadi, Sasan Yazdani
Summary: The research examined the effect of low-temperature calcination on sol-gel derived amorphous alumina coatings, with coatings calcined at 300 degrees C exhibiting significantly improved corrosion resistance compared to those calcined at 500 degrees C.
SURFACE & COATINGS TECHNOLOGY
(2021)
Article
Materials Science, Multidisciplinary
Madeeha Riaz, Manahil Najam, Hina Imtiaz, Farooq Bashir, Tousif Hussain
Summary: This study focuses on the structural and biological analysis of Zn-Cu based biodegradable alloys for orthopedic applications. The results indicate that the alloys have good electrical conductivity and biocompatibility, with potential for promoting bone growth and healing process. Additionally, the alloys exhibit a low corrosion rate and improved corrosion resistance.
MATERIALS CHEMISTRY AND PHYSICS
(2024)
Article
Materials Science, Multidisciplinary
Rijo Rajeev, Sk Safikul Islam, Anitha Varghese, Gurumurthy Hegde, Suryasarathi Bose
Summary: In this study, a facile and selective electrochemical sensor was developed for the sensing of guanosine. The sensor utilized a unique porous structure and ordered framework, enabling linear detection of guanosine concentration in the range of 0.123-720 μM under specific conditions.
MATERIALS CHEMISTRY AND PHYSICS
(2024)
Article
Materials Science, Multidisciplinary
Rafael V. M. Freire, Dominique Celeste de A. Dias, Jose Yago Rodrigues Silva, Dayane Kelly Dias do Nascimento Santos, Larissa T. Jesus, Ricardo O. Freire, Severino A. Junior
Summary: This study reports the extraction and isolation of euphol from nature, its adsorption in nanosized ZIF-8, and the efficacy of this system against cancer cells. Experimental and simulation results show that ZIF-8 can enhance the effectiveness of euphol against cancer cells and selectively target cancer cells.
MATERIALS CHEMISTRY AND PHYSICS
(2024)
Article
Materials Science, Multidisciplinary
Manal A. Awad, Awatif A. Hendi, Maha M. Almoneef, Maymunah Alwehaibi, Khalid M. Ortashi, Wadha Alenazi, Fatimah S. Alfaifi, Shareefa Alahmariye, Asma Alangery, Warda Ali Alghoubiri, Haia Aldosari
Summary: In this study, magnesium-doped zinc oxide nanoparticles were synthesized and characterized. The research findings show that magnesium doping can alter the crystal structure and optical properties of zinc oxide, while enhancing its dielectric constant.
MATERIALS CHEMISTRY AND PHYSICS
(2024)
Article
Materials Science, Multidisciplinary
F. J. Willars-Rodriguez, I. R. Chaverz-Urbiola, M. A. Hernandez-Landaverde, A. Zavala-Franco, E. A. Chavez-Urbiola, P. Vorobiev, Yu V. Vorobiev
Summary: This study focuses on manganese doped CdS thin films synthesized by chemical bath deposition. The incorporation of Mn2+ cations in CdS was found to influence the crystalline structure, morphology, and optoelectronic properties. Doped thin films exhibited a uniform hexagonal structure, changed growth orientation, and showed scale-like and needle-like morphologies. The bandgap and rectification speed of Schottky diodes were modified by introducing manganese. This study suggests the potential for affordable high-speed optoelectronic devices.
MATERIALS CHEMISTRY AND PHYSICS
(2024)
Article
Materials Science, Multidisciplinary
Mehdi Javidi, Hooman Karimi Abadeh, Fatemeh Namazi, Hamid Reza Yazdanpanah, Narjes Shirvani Shiri
Summary: This study investigated the synergistic effect of temperature, solution velocity, and sulphuric acid concentration on the corrosion behavior of carbon steel using response surface methodology. The results showed that temperature affected anodic reactions, solution velocity influenced cathodic reactions, and acid concentration altered the corrosion mechanisms by changing the properties of the surface layer.
MATERIALS CHEMISTRY AND PHYSICS
(2024)
Article
Materials Science, Multidisciplinary
R. Sakthivel, Thirumoorthy Kulandaivel, Kirankumar Venkatesan Savunthari, K. Mohanraj, Hans-Uwe Dahms, Aswin kumar Anbalagan, Manjunath Rangasamy, Kien-Voon Kong
Summary: In this study, saturated fatty acids were incorporated with silane to modify viscose fabric, resulting in superhydrophobic and superoleophilic properties. The modified fabric showed excellent separation efficiency for oil and organic solvents, with high absorption capacity. The modified fabric also exhibited durability and retained its properties in harsh conditions.
MATERIALS CHEMISTRY AND PHYSICS
(2024)
Article
Materials Science, Multidisciplinary
Wei Zhang, Hong Lei, Wenqing Liu, Zefang Zhang, Yi Chen, Xiaogang Hu, Xiangshan Ye
Summary: In this study, EDTA-grafted alumina composite abrasives were produced by a two-step process for the CMP of sapphire substrates. Experimental results showed that the modified abrasives exhibited better dispersion properties and significantly improved polishing efficiency, with higher material removal rates and lower surface roughness. The combination of chemical reaction and mechanical action enhanced the CMP performance.
MATERIALS CHEMISTRY AND PHYSICS
(2024)
Article
Materials Science, Multidisciplinary
Shumaila Rafaqat, Bushra Perveen, Warda Raqba, Warda Imran, Arshad Hussain, Naeem Ali
Summary: This study developed a MnP-based biosensor for quantitative measurement of dye concentrations using electrochemical signals. The effects of two different dyes on MnP activity were investigated, with one dye showing inhibitory effects and the other dye having no effect. The study demonstrates the potential application of enzyme-based biosensors in dye detection and toxicological monitoring.
MATERIALS CHEMISTRY AND PHYSICS
(2024)
Article
Materials Science, Multidisciplinary
Jinyan Shi, Oguzhan Yavuz Bayraktar, Baris Bayrak, Burak Bodur, Ali Oz, Gokhan Kaplan, Abdulkadir Cuneyt Aydin
Summary: The elemental composition of precursors is crucial for the performance development of geopolymers. The use of lime instead of metakaolin increases the fluidity and mechanical properties of geopolymers, while the addition of gypsum decreases them. Furthermore, higher lime content exacerbates the negative effect of gypsum.
MATERIALS CHEMISTRY AND PHYSICS
(2024)
Article
Materials Science, Multidisciplinary
Aayush Gupta, Kaveri Ajravat, Loveleen K. Brar, O. P. Pandey, Pandey Rajagopalan
Summary: This study focuses on the performance of Mn3O4-ZnO composite material in wastewater treatment and energy storage applications, and presents a detailed comparative analysis. Results show that the composite material with equal concentrations of Mn3O4 and ZnO exhibits excellent photocatalytic activity and high capacitance.
MATERIALS CHEMISTRY AND PHYSICS
(2024)
Article
Materials Science, Multidisciplinary
V. Murugabalaji, Matruprasad Rout, Harsh Soni, Biranchi Narayan Sahoo
Summary: This study focuses on the corrosion characteristics of AA 7075 and AA 7075 based hybrid composite fabricated using stir casting and hot rolling techniques. The results show that the hybrid composite produced by hot cross rolling exhibits better corrosion resistance compared to the base metal. The addition of a small amount of graphite improves the bonding between the matrix and reinforcements, and the hot cross rolling enhances this bonding, leading to the formation of a strong passivation oxide layer and increased charge transfer resistance, thereby improving corrosion resistance.
MATERIALS CHEMISTRY AND PHYSICS
(2024)
Article
Materials Science, Multidisciplinary
Fangkun Ning, Qinghao Shi, Shuping Kong, Weitao Jia, Lifeng Ma
Summary: The paper investigates a new method of rolling sheets with variable chamfering amounts in both the transversal and normal directions. The feasibility of the technological process was tested through simulation and compared with experimental results. Three important process parameters, temperature, stress, and flow velocity, were used to evaluate the effects on chamfering amount before determining the optimal angle. The spread formula for evaluating the shape quality of the plate after ECR was obtained through testing and theory.
MATERIALS CHEMISTRY AND PHYSICS
(2024)
Article
Materials Science, Multidisciplinary
Aqeel Abbas, M. A. Hussein, Mohamed Javid
Summary: In this study, the AM60 magnesium alloy was processed using high-energy ball milling, and the results showed that different reinforcement agents had certain effects on particle size, crystallite size, lattice strain, and dislocation density.
MATERIALS CHEMISTRY AND PHYSICS
(2024)
Article
Materials Science, Multidisciplinary
D. S. Mahmoud, E. M. Eldesouki, W. M. Abd El-Gawad
Summary: The development of flexible and lightweight microwave-absorbing materials has become a trendy topic. This study focuses on enhancing the microwave-absorbing performance of butadiene-acrylonitrile rubber (NBR) by incorporating novel reinforcing nanofillers. The results show that the NBR nanocomposite with a loading of 16 parts per hundred rubber (phr) of LiFe 20%/Si has the best microwave-absorbing performance.
MATERIALS CHEMISTRY AND PHYSICS
(2024)